ASTM D5755-2003 用石棉结构值表面负荷用透射电子显微镜对尘埃微真空取样和间接分析的标准试验方法

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【英文标准名称】:StandardTestMethodforMicrovacuumSamplingandIndirectAnalysisofDustbyTransmissionElectronMicroscopyforAsbestosStructureNumberSurfaceLoading
【原文标准名称】:用石棉结构值表面负荷用透射电子显微镜对尘埃微真空取样和间接分析的标准试验方法
【标准号】:ASTMD5755-2003
【标准状态】:现行
【国别】:
【发布日期】:2003
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D22.07
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:分析;试验方法;尘埃;石棉
【英文主题词】:asbestos;microvacuuming;settleddust;TEM
【摘要】:Thismicrovacuumsamplingandindirectanalysismethodisusedforthegeneraltestingofnon-airbornedustsamplesforasbestos.Itisusedtoassistintheevaluationofdustthatmaybefoundonsurfacesinbuildingssuchasceilingtiles,shelving,electricalcomponents,ductwork,carpet,etc.ThistestmethodprovidesanindexofthesurfaceloadingofasbestosstructuresinthedustperunitareaanalyzedasderivedfromaquantitativeTEManalysis.5.1.1Thistestmethoddoesnotdescribeproceduresortechniquesrequiredtoevaluatethesafetyorhabitabilityofbuildingswithasbestos-containingmaterials,orcompliancewithfederal,state,orlocalregulationsorstatutes.Itistheuser’responsibilitytomakethesedeterminations.5.1.2Atpresent,norelationshiphasbeenestablishedbetweenasbestos-containingdustasmeasuredbythistestmethodandpotentialhumanexposuretoairborneasbestos.Accordingly,theusersshouldconsiderotheravailableinformationintheirinterpretationofthedataobtainedfromthistestmethod.Thisdefinitionofdustacceptsallparticlessmallenoughtopassthrougha1mm(No.18)screen.Thus,asingle,largeasbestoscontainingparticle(s)(fromthelargeendoftheparticlesizedistribution)dispersedduringsamplepreparationmayresultinanomalouslylargeasbestossurfaceloadingresultsintheTEManalysesofthatsample.Itis,therefore,recommendedthatmultipleindependentsamplesaresecuredfromthesamearea,andthataminimumofthreesamplesbeanalyzedbytheentireprocedure.1.1Thistestmethodcoversaprocedureto(a)identifyasbestosindustand(b)provideanestimateofthesurfaceloadingofasbestosinthesampleddustreportedasthenumberofasbestosstructuresperunitareaofsampledsurface.1.1.1Ifanestimateoftheasbestosmassistobedetermined,theuserisreferredtoTestMethodD5756.1.2Thistestmethoddescribestheequipmentandproceduresnecessaryforsampling,byamicrovacuumtechnique,non-airbornedustforlevelsofasbestosstructures.Thenon-airbornesampleiscollectedinsideastandardfiltermembranecassettefromthesamplingofasurfaceareafordustwhichmaycontainasbestos.1.2.1Thisprocedureusesamicrovacuumingsamplingtechnique.Thecollectionefficiencyofthistechniqueisunknownandwillvaryamongsubstrates.Propertiesinfluencingcollectionefficiencyincludesurfacetexture,adhesiveness,electrostaticpropertiesandotherfactors.1.3Asbestosidentifiedbytransmissionelectronmicroscopy(TEM)isbasedonmorphology,selectedareaelectrondiffraction(SAED),andenergydispersiveX-rayanalysis(EDXA).Someinformationaboutstructuresizeisalsodetermined.1.4Thistestmethodisgenerallyapplicableforanestimateofthesurfaceloadingofasbestosstructuresstartingfromapproximately1000asbestosstructurespersquarecentimetre.1.4.1Theprocedureoutlinedinthistestmethodemploysanindirectsamplepreparationtechnique.Itisintendedtodisperseaggregatedasbestosintofundamentalfibrils,fiberbundles,clusters,ormatricesthatcanbemoreaccuratelyquantifiedbytransmissionelectronmicroscopy.However,aswithallindirectsamplepreparationtechniques,theasbestosobservedforquantificationmaynotrepresentthephysicalformoftheasbestosassampled.Morespecifically,theproceduredescribedneithercreatesnordestroysasbestos,butitmayalterthephysicalformofthemineralfibers.1.5ThevaluesstatedinSIunitsaretoberegardedasthestandard.Thevaluesgiveninparenthesesareforinformationonly.1.6Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishapp......
【中国标准分类号】:P09;C51
【国际标准分类号】:13_040_20
【页数】:13P.;A4
【正文语种】: